Instrument Specification
A 3-channel NMR spectrometer equipped with a 3-channel gradient amplifier, equipped with the following, for either solution state, solid state or microimaging studies:
For spectroscopy, solution NMR studies:
- 5 mm 1H selective probe
- 10 mm automatic QNP probe, computer switchable for 1H, 15N, 31P and 13C nuclei.
- 10 mm automatic QNP probe, computer switchable for 1H, 19F and 31P nuclei.
- 8 mm triple-resonance (1H, 15N, 13C), inverse probe (TXI).
- A ‘boron-free’ probe for 10B and 11B spectroscopy
For solid-state NMR, MAS studies:
- 1.3 mm DVT multinuclear double resonance 15N-31P/19F-1H probe (1.7 microL active volume, 67 kHz spinning speed, VT range -30C to 70C)
- 2.5 mm top-loading DVT multinuclear triple resonance X/Y/19F-1H (8 microL (14 fir thin-walled rotors) active volume, 35 kHz spinning speed, VT range -50C to 80C)
- 4 mm top-loading DVT multinuclear triple resonance X/Y/19F-1H probe (50 microL active volume, 15 kHz spinning speed, VT range -130C to 150C)
For imaging studies:
- 5 mm microscopy probe that includes actively shielded gradients (up to 200 G/cm) with RF coils for 1H, 1H/13C, and 1H/31P.
- A mini-imaging probe with actively shielded gradients (up to 150 G/cm) that includes several 1H RF coils, with diameters between 4 and 30 mm.
Location
Wolf building
Staff Contacts
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Dr. Talia Harris
Staff Scientist